- published: 30 Mar 2016
- views: 6612
-
remove the playlistPhosphoros Trial
- remove the playlistPhosphoros Trial
back to playlist
How to make white phosphorus - Trial 1 for record. Using a mix of NaPO3, Al + Si02 (cat litter). I successfully synthesize a small amount during & after the reaction but it's clear that my distiller needs a new all steel design.
how to make white phosphorus
white phosphorus synthesis
make phosphorus at home
how to make P4
the synthesis of white phosphorus
elemental phosphorus
https://en.wikipedia.org/wiki/Phosphorus
There is not much great info on the topic of making white phosphorus. I looked far and found a few things but nothing that appeased my value of education and everything that comes along with making my favorite element.
As an element white phosphorus has many awesome properties! It is the only element in the world that "naturally glows." That is in normal conditions in it's normal state.
Something about that, non-spiritual, without all the god, without all the religion.... it is an element that glows when you turn the lights out. It does this because it wants to burn into something different. And humans are exactly the same. We spend our whole lives trying to be someone different. Different. Phosphorus is very different.... ,
Like sulfurs homicidally evil light bearing twin. It can kill you. If that makes sense. It also causes algae blooms, life, it's lipid soluble and will melt into your skin or fat or anything else oily and burn and dissolve it's way through as you shriek in agony.
From a safety standpoint, you'd be MUCH HEALTHIER squeezing a raw ball of sodium with wet hands. Not that I suggest you do. What I'm saying is P4 is very toxic which is why it's "magical" reaction isn't demonstrated much in science classrooms. We will burn iron in oxygen blow things out of cannons but chemists and this not so safe. Only you can answer that question.
However, I believe low levels (sub 10gm levels) with proper ventilation and a copper sulfate sprayed appropriate gas respirator scrubber on your chrome dome fool is definitely safe. I know my scrubber looks dirty but that's a custom made 3 stage security filter. Charcoal wrapped polyester filters (the preinstalled filters that come with it). Then there's another open and wider area of activated charcoal (fishtank) and copper sulfate sprayed on the inner and outer polyester layer. I attach a 3" rubber gutter piece from Lowes for the big extension from regular masks. If you ever build a custom mask to make white phosphorus with do not fool yourself that you don't need ventilation. You do. Just don't try this at home unless you know what you're doing.
My goal is to test more ways of making white phosphorus. I want to try production and reducing with Al/Mg/C or Al/Mg or Al/C or zinc or anything safe to measure yield. My next trial will be filmed and edited much better. I can narrate much better with a microphone than my gas mask on a camera I returned 1 week ago.
So expect me making more videos of white phosphorus.
https://en.wikipedia.org/wiki/White_p...
In summation....
Brass to steel does not work. I chose brass simply because I wanted a smaller distiller. I thought it would work better due to more surface area. But my observation is when white p is liberated the molten liquid is very hot, fresh and wants to react with everything. I believe the bit of zinc in brass acts as a "magnet" to attract the phosphorus. So it skins up with a layer of zinc and (or) copper sulfide. Then inside it just sticks almost like tar.
So a change to all steel and tar are the 2 main things I learned in this experiment.
When you create white phosphorus it behaves like tar. Using an inert gas would most likely prevent this "liquid sticky" oxygen exposed material. That's what makes it stick it's the O2.
I must create more and better videos on this element. Where I slowly scale up into a forge built for a retort that has the main pipe, elbow and half the distiller sticking out the door of the forge. With a vent hole above it. This will disperse very hot to almost 3/4 of the whole retort and vaporize distill the P4 straight to water. I will update with more videos so stay tuned! btw sry bout dat body hare.
The failure recently i had while trying to make P4 got me to further research the method and i was basically overthinking it. it did not need super strong welded retort afterall nor did the brute force attempt at heating seem needed. slow and steady won the race.
Some changes were: the retort obviously, thin walled can with a vertical outlet. using dark Aluminium powder, very finely grinding and well combining of the reagents, flushing the retort with Argon, monitoring the temperature and attempting to control it, using warm water in the receiver.
It worked well. the only thing annoying was the amount of P4 vapour burning up- i could see the flames had the greenish colour of lost product! the camera barely picks it up but just in some frames.
Never the less it did work and is repeatable and able to be scaled up so I'm pleased. after a couple more runs when i have a bit more i will
do a video on cleaning it up to a nice white product.
See more on Bitchute:
https://www.bitchute.com/profile/4uBPC9RCH6e9/
And minds: https://www.minds.com/EnergyUnleashed
- published: 12 Jun 2017
- views: 18970
basically a test run of a procedure i found which is a micro scale run to make White phosphorus. the original publisher cited this equation :
6NaPO3 + 10AI + 3Si02 = 3Na2Si03 + 5Al203 + 3P2
which was first published over a century ago by j.franck.
The publisher cited a 50% yield of 250mg out of the 500mg available P which was reportedly re sublimed to separate the white from the red P.
these two runs were basically a test run to prove the concept for myself and to see how the reaction proceeds before i scale it up with a steel retort . it seems to have worked very well and at a much lower temperature than i thought.
Experimental:
3g of a stochiometric ratio of sodium hexametaphosphate,
silicon dioxide and dark aluminium powder in slight excess were
well dried in an oven and mixed thoroughly in a plastic tub.
Exactly 3g of this mixture was placed in an 18mm Test tube
and this was sealed with a stopper which i had bored with two holes, one for argon to be inlet and one for a bent glass leading into cold water. paper toweling was wrapped around the tube and wet with ice water. the tube was then heated with a butane torch firstly and a MAPP torch for the second attempt.
the second attempt worked better.
I was able to get a little product recovered -i did not weigh it and watched it burn. but this was pretty much a test run with bigger and better attempts to come.
- published: 27 Mar 2017
- views: 6388
All the white Phosphorus i have made so far was cleaned using similar methods to what is used in industrial process- using dilute dichromate in acidic solutions.
i made a small solution of potassium dichromate with sulfuric acid and added some of this to the molten P4 while stirring the solution. The amount of dichromate solution and time it was immersed was quite arbitrary and i added as much as i thought i would need- a few mls and kept the cleaning going until i though it looked clean enough.
eventually it turned out much cleaner than i started, being a nice pale yellow colour rather than the red i started with.
Next i may do a video on converting some of this to red phosphorus.
maybe. it is becoming wintery here.
See more on Bitchute:
https://www.bitchute.com/profile/4uBPC9RCH6e9/
And minds: https://www.minds.com/EnergyUnleashed
Music:
Destination Unknown by Audionautix is licensed under a Creative Commons Attribution license (https://creativecommons.org/licenses/by/4.0/)
Artist: http://audionautix.com/
Impact Intermezzo by Kevin MacLeod is licensed under a Creative Commons Attribution license (https://creativecommons.org/licenses/by/4.0/)
Source: http://incompetech.com/music/royalty-free/index.html?isrc=USUAN1100620
Artist: http://incompetech.com/
- published: 20 Jun 2017
- views: 6284
Jameson Quinn of Quinn Farms in Cove City, NC accidentally left Genesis Ag's Liberate off of 16 rows during the transplant process on April 4th. By May 19th the visual results in his field were almost unbelievable.
To learn more about Genesis Ag's liberate go here:
http://www.genesis.ag/products/liberate/
- published: 19 May 2016
- views: 2163
developed with YouTube
Trial
In law, a trial is a coming together of parties to a dispute, to present information (in the form of evidence) in a tribunal, a formal setting with the authority to adjudicate claims or disputes. One form of tribunal is a court. The tribunal, which may occur before a judge, jury, or other designated trier of fact, aims to achieve a resolution to their dispute.
Types of trial divided by the finder of fact
Where the trial is held before a group of members of the community, it is called a jury trial. Where the trial is held solely before a judge, it is called a bench trial.
Bench trials are often resolved faster. Furthermore, a favorable ruling for one party in a bench trial will frequently lead the other party to offer a settlement.
Hearings before administrative bodies may have many of the features of a trial before a court, but are typically not referred to as trials.
An appellate proceeding is also generally not deemed a trial, because such proceedings are usually restricted to review of the evidence presented before the trial court, and do not permit the introduction of new evidence.
This page contains text from Wikipedia, the Free Encyclopedia - https://wn.com/Trial
List of Batman: The Animated Series episodes
Batman: The Animated Series is an American television series based on the DC Comics superhero Batman, which was produced by Warner Bros. Animation and originally aired on Fox from 1992 to 1995; lasting 85 episodes. The series has since aired in re-runs on various other broadcast and cable networks, including The WB, Cartoon Network, Toon Disney and The Hub. Each episode is approximately 22 minutes long, excluding commercials.
The series is part of what has become known as the DC animated universe, which consists of eight animated television shows and four animated films, largely surrounding DC Comics characters and their respective mythos. This includes Superman: The Animated Series, The New Batman Adventures, Batman Beyond, Static Shock, The Zeta Project, Justice League and Justice League Unlimited.
Episode list
This article lists the episodes in their production order, in accordance with the order the series was released on DVD; rather than by their original airdates, the former was often preferred by fans due to establishment, story flow, consistency, character introduction, etc.
This page contains text from Wikipedia, the Free Encyclopedia - https://wn.com/List_of_Batman:_The_Animated_Series_episodes
American Association for Justice
The American Association for Justice (AAJ), formerly the Association of Trial Lawyers of America (ATLA) is a nonprofit advocacy and lobbying organization for plaintiff's lawyers in the United States. AAJ's stated mission is to "promote a fair and effective justice system." Focused on opposing tort reform, the organization is one of the Democratic Party's most influential political allies.
History
In 1946, a group of plaintiffs' attorneys involved in workers' compensation litigation founded the National Association of Claimants' Compensation Attorneys (NACCA). As their work broadened beyond workers' compensation, in 1960 the NACCA changed its name to the National Association of Claimants' Counsel of America, and four years later, to the American Trial Lawyers Association. In 1972, these groups merged as the Association of Trial Lawyers of America (ATLA). In 1977, ATLA's headquarters moved from Boston to Washington, D.C.
In 2006, ATLA became the American Association for Justice (AAJ). Around the same time, a group of attorneys quietly began forming a competitor organization to AAJ. The competitor organization called itself The American Trial Lawyers Association, or TheATLA. TheATLA solicited thousands of AAJ's members to join. AAJ filed suit to force TheATLA to drop the name, arguing it was confusing AAJ members and infringing a trademark held by AAJ.
This page contains text from Wikipedia, the Free Encyclopedia - https://wn.com/American_Association_for_Justice
Podcasts:
-
How To Make White Phosphorus (Trial 1)
How to make white phosphorus - Trial 1 for record. Using a mix of NaPO3, Al + Si02 (cat litter). I successfully synthesize a small amount during & after the reaction but it's clear that my distiller needs a new all steel design. how to make white phosphorus white phosphorus synthesis make phosphorus at home how to make P4 the synthesis of white phosphorus elemental phosphorus https://en.wikipedia.org/wiki/Phosphorus There is not much great info on the topic of making white phosphorus. I looked far and found a few things but nothing that appeased my value of education and everything that comes along with making my favorite element. As an element white phosphorus has many awesome properties! It is the only element in the world that "naturally glows." That is in normal conditions in it's ...
published: 30 Mar 2016 -
Making White Phosphorus- done it this time!
The failure recently i had while trying to make P4 got me to further research the method and i was basically overthinking it. it did not need super strong welded retort afterall nor did the brute force attempt at heating seem needed. slow and steady won the race. Some changes were: the retort obviously, thin walled can with a vertical outlet. using dark Aluminium powder, very finely grinding and well combining of the reagents, flushing the retort with Argon, monitoring the temperature and attempting to control it, using warm water in the receiver. It worked well. the only thing annoying was the amount of P4 vapour burning up- i could see the flames had the greenish colour of lost product! the camera barely picks it up but just in some frames. Never the less it did work and is repeatable...
published: 12 Jun 2017 -
Making White Phosphorus -01 Testing the concept
basically a test run of a procedure i found which is a micro scale run to make White phosphorus. the original publisher cited this equation : 6NaPO3 + 10AI + 3Si02 = 3Na2Si03 + 5Al203 + 3P2 which was first published over a century ago by j.franck. The publisher cited a 50% yield of 250mg out of the 500mg available P which was reportedly re sublimed to separate the white from the red P. these two runs were basically a test run to prove the concept for myself and to see how the reaction proceeds before i scale it up with a steel retort . it seems to have worked very well and at a much lower temperature than i thought. Experimental: 3g of a stochiometric ratio of sodium hexametaphosphate, silicon dioxide and dark aluminium powder in slight excess were well dried in an oven and mixed thor...
published: 27 Mar 2017 -
Cleaning the white Phosphorus.
All the white Phosphorus i have made so far was cleaned using similar methods to what is used in industrial process- using dilute dichromate in acidic solutions. i made a small solution of potassium dichromate with sulfuric acid and added some of this to the molten P4 while stirring the solution. The amount of dichromate solution and time it was immersed was quite arbitrary and i added as much as i thought i would need- a few mls and kept the cleaning going until i though it looked clean enough. eventually it turned out much cleaner than i started, being a nice pale yellow colour rather than the red i started with. Next i may do a video on converting some of this to red phosphorus. maybe. it is becoming wintery here. See more on Bitchute: https://www.bitchute.com/profile/4uBPC9RCH6e...
published: 20 Jun 2017 -
Jawdropping Side by Side Trial with Genesis Ag Liberate
Jameson Quinn of Quinn Farms in Cove City, NC accidentally left Genesis Ag's Liberate off of 16 rows during the transplant process on April 4th. By May 19th the visual results in his field were almost unbelievable. To learn more about Genesis Ag's liberate go here: http://www.genesis.ag/products/liberate/
published: 19 May 2016
developed with YouTube
12:11
How To Make White Phosphorus (Trial 1)
- Order: Reorder
- Duration: 12:11
- Uploaded Date: 30 Mar 2016
- views: 6612
How to make white phosphorus - Trial 1 for record. Using a mix of NaPO3, Al + Si02 (cat litter). I successfully synthesize a small amount during & after the rea...
How to make white phosphorus - Trial 1 for record. Using a mix of NaPO3, Al + Si02 (cat litter). I successfully synthesize a small amount during & after the reaction but it's clear that my distiller needs a new all steel design.
how to make white phosphorus
white phosphorus synthesis
make phosphorus at home
how to make P4
the synthesis of white phosphorus
elemental phosphorus
https://en.wikipedia.org/wiki/Phosphorus
There is not much great info on the topic of making white phosphorus. I looked far and found a few things but nothing that appeased my value of education and everything that comes along with making my favorite element.
As an element white phosphorus has many awesome properties! It is the only element in the world that "naturally glows." That is in normal conditions in it's normal state.
Something about that, non-spiritual, without all the god, without all the religion.... it is an element that glows when you turn the lights out. It does this because it wants to burn into something different. And humans are exactly the same. We spend our whole lives trying to be someone different. Different. Phosphorus is very different.... ,
Like sulfurs homicidally evil light bearing twin. It can kill you. If that makes sense. It also causes algae blooms, life, it's lipid soluble and will melt into your skin or fat or anything else oily and burn and dissolve it's way through as you shriek in agony.
From a safety standpoint, you'd be MUCH HEALTHIER squeezing a raw ball of sodium with wet hands. Not that I suggest you do. What I'm saying is P4 is very toxic which is why it's "magical" reaction isn't demonstrated much in science classrooms. We will burn iron in oxygen blow things out of cannons but chemists and this not so safe. Only you can answer that question.
However, I believe low levels (sub 10gm levels) with proper ventilation and a copper sulfate sprayed appropriate gas respirator scrubber on your chrome dome fool is definitely safe. I know my scrubber looks dirty but that's a custom made 3 stage security filter. Charcoal wrapped polyester filters (the preinstalled filters that come with it). Then there's another open and wider area of activated charcoal (fishtank) and copper sulfate sprayed on the inner and outer polyester layer. I attach a 3" rubber gutter piece from Lowes for the big extension from regular masks. If you ever build a custom mask to make white phosphorus with do not fool yourself that you don't need ventilation. You do. Just don't try this at home unless you know what you're doing.
My goal is to test more ways of making white phosphorus. I want to try production and reducing with Al/Mg/C or Al/Mg or Al/C or zinc or anything safe to measure yield. My next trial will be filmed and edited much better. I can narrate much better with a microphone than my gas mask on a camera I returned 1 week ago.
So expect me making more videos of white phosphorus.
https://en.wikipedia.org/wiki/White_p...
In summation....
Brass to steel does not work. I chose brass simply because I wanted a smaller distiller. I thought it would work better due to more surface area. But my observation is when white p is liberated the molten liquid is very hot, fresh and wants to react with everything. I believe the bit of zinc in brass acts as a "magnet" to attract the phosphorus. So it skins up with a layer of zinc and (or) copper sulfide. Then inside it just sticks almost like tar.
So a change to all steel and tar are the 2 main things I learned in this experiment.
When you create white phosphorus it behaves like tar. Using an inert gas would most likely prevent this "liquid sticky" oxygen exposed material. That's what makes it stick it's the O2.
I must create more and better videos on this element. Where I slowly scale up into a forge built for a retort that has the main pipe, elbow and half the distiller sticking out the door of the forge. With a vent hole above it. This will disperse very hot to almost 3/4 of the whole retort and vaporize distill the P4 straight to water. I will update with more videos so stay tuned! btw sry bout dat body hare.
https://wn.com/How_To_Make_White_Phosphorus_(Trial_1)
How to make white phosphorus - Trial 1 for record. Using a mix of NaPO3, Al + Si02 (cat litter). I successfully synthesize a small amount during & after the reaction but it's clear that my distiller needs a new all steel design.
how to make white phosphorus
white phosphorus synthesis
make phosphorus at home
how to make P4
the synthesis of white phosphorus
elemental phosphorus
https://en.wikipedia.org/wiki/Phosphorus
There is not much great info on the topic of making white phosphorus. I looked far and found a few things but nothing that appeased my value of education and everything that comes along with making my favorite element.
As an element white phosphorus has many awesome properties! It is the only element in the world that "naturally glows." That is in normal conditions in it's normal state.
Something about that, non-spiritual, without all the god, without all the religion.... it is an element that glows when you turn the lights out. It does this because it wants to burn into something different. And humans are exactly the same. We spend our whole lives trying to be someone different. Different. Phosphorus is very different.... ,
Like sulfurs homicidally evil light bearing twin. It can kill you. If that makes sense. It also causes algae blooms, life, it's lipid soluble and will melt into your skin or fat or anything else oily and burn and dissolve it's way through as you shriek in agony.
From a safety standpoint, you'd be MUCH HEALTHIER squeezing a raw ball of sodium with wet hands. Not that I suggest you do. What I'm saying is P4 is very toxic which is why it's "magical" reaction isn't demonstrated much in science classrooms. We will burn iron in oxygen blow things out of cannons but chemists and this not so safe. Only you can answer that question.
However, I believe low levels (sub 10gm levels) with proper ventilation and a copper sulfate sprayed appropriate gas respirator scrubber on your chrome dome fool is definitely safe. I know my scrubber looks dirty but that's a custom made 3 stage security filter. Charcoal wrapped polyester filters (the preinstalled filters that come with it). Then there's another open and wider area of activated charcoal (fishtank) and copper sulfate sprayed on the inner and outer polyester layer. I attach a 3" rubber gutter piece from Lowes for the big extension from regular masks. If you ever build a custom mask to make white phosphorus with do not fool yourself that you don't need ventilation. You do. Just don't try this at home unless you know what you're doing.
My goal is to test more ways of making white phosphorus. I want to try production and reducing with Al/Mg/C or Al/Mg or Al/C or zinc or anything safe to measure yield. My next trial will be filmed and edited much better. I can narrate much better with a microphone than my gas mask on a camera I returned 1 week ago.
So expect me making more videos of white phosphorus.
https://en.wikipedia.org/wiki/White_p...
In summation....
Brass to steel does not work. I chose brass simply because I wanted a smaller distiller. I thought it would work better due to more surface area. But my observation is when white p is liberated the molten liquid is very hot, fresh and wants to react with everything. I believe the bit of zinc in brass acts as a "magnet" to attract the phosphorus. So it skins up with a layer of zinc and (or) copper sulfide. Then inside it just sticks almost like tar.
So a change to all steel and tar are the 2 main things I learned in this experiment.
When you create white phosphorus it behaves like tar. Using an inert gas would most likely prevent this "liquid sticky" oxygen exposed material. That's what makes it stick it's the O2.
I must create more and better videos on this element. Where I slowly scale up into a forge built for a retort that has the main pipe, elbow and half the distiller sticking out the door of the forge. With a vent hole above it. This will disperse very hot to almost 3/4 of the whole retort and vaporize distill the P4 straight to water. I will update with more videos so stay tuned! btw sry bout dat body hare.
- published: 30 Mar 2016
- views: 6612
8:18
Making White Phosphorus- done it this time!
- Order: Reorder
- Duration: 8:18
- Uploaded Date: 12 Jun 2017
- views: 18970
The failure recently i had while trying to make P4 got me to further research the method and i was basically overthinking it. it did not need super strong welde...
The failure recently i had while trying to make P4 got me to further research the method and i was basically overthinking it. it did not need super strong welded retort afterall nor did the brute force attempt at heating seem needed. slow and steady won the race.
Some changes were: the retort obviously, thin walled can with a vertical outlet. using dark Aluminium powder, very finely grinding and well combining of the reagents, flushing the retort with Argon, monitoring the temperature and attempting to control it, using warm water in the receiver.
It worked well. the only thing annoying was the amount of P4 vapour burning up- i could see the flames had the greenish colour of lost product! the camera barely picks it up but just in some frames.
Never the less it did work and is repeatable and able to be scaled up so I'm pleased. after a couple more runs when i have a bit more i will
do a video on cleaning it up to a nice white product.
See more on Bitchute:
https://www.bitchute.com/profile/4uBPC9RCH6e9/
And minds: https://www.minds.com/EnergyUnleashed
https://wn.com/Making_White_Phosphorus_Done_It_This_Time
The failure recently i had while trying to make P4 got me to further research the method and i was basically overthinking it. it did not need super strong welded retort afterall nor did the brute force attempt at heating seem needed. slow and steady won the race.
Some changes were: the retort obviously, thin walled can with a vertical outlet. using dark Aluminium powder, very finely grinding and well combining of the reagents, flushing the retort with Argon, monitoring the temperature and attempting to control it, using warm water in the receiver.
It worked well. the only thing annoying was the amount of P4 vapour burning up- i could see the flames had the greenish colour of lost product! the camera barely picks it up but just in some frames.
Never the less it did work and is repeatable and able to be scaled up so I'm pleased. after a couple more runs when i have a bit more i will
do a video on cleaning it up to a nice white product.
See more on Bitchute:
https://www.bitchute.com/profile/4uBPC9RCH6e9/
And minds: https://www.minds.com/EnergyUnleashed
- published: 12 Jun 2017
- views: 18970
5:33
Making White Phosphorus -01 Testing the concept
- Order: Reorder
- Duration: 5:33
- Uploaded Date: 27 Mar 2017
- views: 6388
basically a test run of a procedure i found which is a micro scale run to make White phosphorus. the original publisher cited this equation :
6NaPO3 + 10AI + 3...
basically a test run of a procedure i found which is a micro scale run to make White phosphorus. the original publisher cited this equation :
6NaPO3 + 10AI + 3Si02 = 3Na2Si03 + 5Al203 + 3P2
which was first published over a century ago by j.franck.
The publisher cited a 50% yield of 250mg out of the 500mg available P which was reportedly re sublimed to separate the white from the red P.
these two runs were basically a test run to prove the concept for myself and to see how the reaction proceeds before i scale it up with a steel retort . it seems to have worked very well and at a much lower temperature than i thought.
Experimental:
3g of a stochiometric ratio of sodium hexametaphosphate,
silicon dioxide and dark aluminium powder in slight excess were
well dried in an oven and mixed thoroughly in a plastic tub.
Exactly 3g of this mixture was placed in an 18mm Test tube
and this was sealed with a stopper which i had bored with two holes, one for argon to be inlet and one for a bent glass leading into cold water. paper toweling was wrapped around the tube and wet with ice water. the tube was then heated with a butane torch firstly and a MAPP torch for the second attempt.
the second attempt worked better.
I was able to get a little product recovered -i did not weigh it and watched it burn. but this was pretty much a test run with bigger and better attempts to come.
https://wn.com/Making_White_Phosphorus_01_Testing_The_Concept
basically a test run of a procedure i found which is a micro scale run to make White phosphorus. the original publisher cited this equation :
6NaPO3 + 10AI + 3Si02 = 3Na2Si03 + 5Al203 + 3P2
which was first published over a century ago by j.franck.
The publisher cited a 50% yield of 250mg out of the 500mg available P which was reportedly re sublimed to separate the white from the red P.
these two runs were basically a test run to prove the concept for myself and to see how the reaction proceeds before i scale it up with a steel retort . it seems to have worked very well and at a much lower temperature than i thought.
Experimental:
3g of a stochiometric ratio of sodium hexametaphosphate,
silicon dioxide and dark aluminium powder in slight excess were
well dried in an oven and mixed thoroughly in a plastic tub.
Exactly 3g of this mixture was placed in an 18mm Test tube
and this was sealed with a stopper which i had bored with two holes, one for argon to be inlet and one for a bent glass leading into cold water. paper toweling was wrapped around the tube and wet with ice water. the tube was then heated with a butane torch firstly and a MAPP torch for the second attempt.
the second attempt worked better.
I was able to get a little product recovered -i did not weigh it and watched it burn. but this was pretty much a test run with bigger and better attempts to come.
- published: 27 Mar 2017
- views: 6388
5:37
Cleaning the white Phosphorus.
- Order: Reorder
- Duration: 5:37
- Uploaded Date: 20 Jun 2017
- views: 6284
All the white Phosphorus i have made so far was cleaned using similar methods to what is used in industrial process- using dilute dichromate in acidic solutio...
All the white Phosphorus i have made so far was cleaned using similar methods to what is used in industrial process- using dilute dichromate in acidic solutions.
i made a small solution of potassium dichromate with sulfuric acid and added some of this to the molten P4 while stirring the solution. The amount of dichromate solution and time it was immersed was quite arbitrary and i added as much as i thought i would need- a few mls and kept the cleaning going until i though it looked clean enough.
eventually it turned out much cleaner than i started, being a nice pale yellow colour rather than the red i started with.
Next i may do a video on converting some of this to red phosphorus.
maybe. it is becoming wintery here.
See more on Bitchute:
https://www.bitchute.com/profile/4uBPC9RCH6e9/
And minds: https://www.minds.com/EnergyUnleashed
Music:
Destination Unknown by Audionautix is licensed under a Creative Commons Attribution license (https://creativecommons.org/licenses/by/4.0/)
Artist: http://audionautix.com/
Impact Intermezzo by Kevin MacLeod is licensed under a Creative Commons Attribution license (https://creativecommons.org/licenses/by/4.0/)
Source: http://incompetech.com/music/royalty-free/index.html?isrc=USUAN1100620
Artist: http://incompetech.com/
https://wn.com/Cleaning_The_White_Phosphorus.
All the white Phosphorus i have made so far was cleaned using similar methods to what is used in industrial process- using dilute dichromate in acidic solutions.
i made a small solution of potassium dichromate with sulfuric acid and added some of this to the molten P4 while stirring the solution. The amount of dichromate solution and time it was immersed was quite arbitrary and i added as much as i thought i would need- a few mls and kept the cleaning going until i though it looked clean enough.
eventually it turned out much cleaner than i started, being a nice pale yellow colour rather than the red i started with.
Next i may do a video on converting some of this to red phosphorus.
maybe. it is becoming wintery here.
See more on Bitchute:
https://www.bitchute.com/profile/4uBPC9RCH6e9/
And minds: https://www.minds.com/EnergyUnleashed
Music:
Destination Unknown by Audionautix is licensed under a Creative Commons Attribution license (https://creativecommons.org/licenses/by/4.0/)
Artist: http://audionautix.com/
Impact Intermezzo by Kevin MacLeod is licensed under a Creative Commons Attribution license (https://creativecommons.org/licenses/by/4.0/)
Source: http://incompetech.com/music/royalty-free/index.html?isrc=USUAN1100620
Artist: http://incompetech.com/
- published: 20 Jun 2017
- views: 6284
0:26
Jawdropping Side by Side Trial with Genesis Ag Liberate
- Order: Reorder
- Duration: 0:26
- Uploaded Date: 19 May 2016
- views: 2163
Jameson Quinn of Quinn Farms in Cove City, NC accidentally left Genesis Ag's Liberate off of 16 rows during the transplant process on April 4th. By May 19th th...
Jameson Quinn of Quinn Farms in Cove City, NC accidentally left Genesis Ag's Liberate off of 16 rows during the transplant process on April 4th. By May 19th the visual results in his field were almost unbelievable.
To learn more about Genesis Ag's liberate go here:
http://www.genesis.ag/products/liberate/
https://wn.com/Jawdropping_Side_By_Side_Trial_With_Genesis_Ag_Liberate
Jameson Quinn of Quinn Farms in Cove City, NC accidentally left Genesis Ag's Liberate off of 16 rows during the transplant process on April 4th. By May 19th the visual results in his field were almost unbelievable.
To learn more about Genesis Ag's liberate go here:
http://www.genesis.ag/products/liberate/
- published: 19 May 2016
- views: 2163
12:11
How To Make White Phosphorus (Trial 1)
How to make white phosphorus - Trial 1 for record. Using a mix of NaPO3, Al + Si02 (cat li...
published: 30 Mar 2016
How To Make White Phosphorus (Trial 1)
How To Make White Phosphorus (Trial 1)
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- published: 30 Mar 2016
- views: 6612
How to make white phosphorus - Trial 1 for record. Using a mix of NaPO3, Al + Si02 (cat litter). I successfully synthesize a small amount during & after the reaction but it's clear that my distiller needs a new all steel design.
how to make white phosphorus
white phosphorus synthesis
make phosphorus at home
how to make P4
the synthesis of white phosphorus
elemental phosphorus
https://en.wikipedia.org/wiki/Phosphorus
There is not much great info on the topic of making white phosphorus. I looked far and found a few things but nothing that appeased my value of education and everything that comes along with making my favorite element.
As an element white phosphorus has many awesome properties! It is the only element in the world that "naturally glows." That is in normal conditions in it's normal state.
Something about that, non-spiritual, without all the god, without all the religion.... it is an element that glows when you turn the lights out. It does this because it wants to burn into something different. And humans are exactly the same. We spend our whole lives trying to be someone different. Different. Phosphorus is very different.... ,
Like sulfurs homicidally evil light bearing twin. It can kill you. If that makes sense. It also causes algae blooms, life, it's lipid soluble and will melt into your skin or fat or anything else oily and burn and dissolve it's way through as you shriek in agony.
From a safety standpoint, you'd be MUCH HEALTHIER squeezing a raw ball of sodium with wet hands. Not that I suggest you do. What I'm saying is P4 is very toxic which is why it's "magical" reaction isn't demonstrated much in science classrooms. We will burn iron in oxygen blow things out of cannons but chemists and this not so safe. Only you can answer that question.
However, I believe low levels (sub 10gm levels) with proper ventilation and a copper sulfate sprayed appropriate gas respirator scrubber on your chrome dome fool is definitely safe. I know my scrubber looks dirty but that's a custom made 3 stage security filter. Charcoal wrapped polyester filters (the preinstalled filters that come with it). Then there's another open and wider area of activated charcoal (fishtank) and copper sulfate sprayed on the inner and outer polyester layer. I attach a 3" rubber gutter piece from Lowes for the big extension from regular masks. If you ever build a custom mask to make white phosphorus with do not fool yourself that you don't need ventilation. You do. Just don't try this at home unless you know what you're doing.
My goal is to test more ways of making white phosphorus. I want to try production and reducing with Al/Mg/C or Al/Mg or Al/C or zinc or anything safe to measure yield. My next trial will be filmed and edited much better. I can narrate much better with a microphone than my gas mask on a camera I returned 1 week ago.
So expect me making more videos of white phosphorus.
https://en.wikipedia.org/wiki/White_p...
In summation....
Brass to steel does not work. I chose brass simply because I wanted a smaller distiller. I thought it would work better due to more surface area. But my observation is when white p is liberated the molten liquid is very hot, fresh and wants to react with everything. I believe the bit of zinc in brass acts as a "magnet" to attract the phosphorus. So it skins up with a layer of zinc and (or) copper sulfide. Then inside it just sticks almost like tar.
So a change to all steel and tar are the 2 main things I learned in this experiment.
When you create white phosphorus it behaves like tar. Using an inert gas would most likely prevent this "liquid sticky" oxygen exposed material. That's what makes it stick it's the O2.
I must create more and better videos on this element. Where I slowly scale up into a forge built for a retort that has the main pipe, elbow and half the distiller sticking out the door of the forge. With a vent hole above it. This will disperse very hot to almost 3/4 of the whole retort and vaporize distill the P4 straight to water. I will update with more videos so stay tuned! btw sry bout dat body hare.
8:18
Making White Phosphorus- done it this time!
The failure recently i had while trying to make P4 got me to further research the method a...
published: 12 Jun 2017
Making White Phosphorus- done it this time!
Making White Phosphorus- done it this time!
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- published: 12 Jun 2017
- views: 18970
The failure recently i had while trying to make P4 got me to further research the method and i was basically overthinking it. it did not need super strong welded retort afterall nor did the brute force attempt at heating seem needed. slow and steady won the race.
Some changes were: the retort obviously, thin walled can with a vertical outlet. using dark Aluminium powder, very finely grinding and well combining of the reagents, flushing the retort with Argon, monitoring the temperature and attempting to control it, using warm water in the receiver.
It worked well. the only thing annoying was the amount of P4 vapour burning up- i could see the flames had the greenish colour of lost product! the camera barely picks it up but just in some frames.
Never the less it did work and is repeatable and able to be scaled up so I'm pleased. after a couple more runs when i have a bit more i will
do a video on cleaning it up to a nice white product.
See more on Bitchute:
https://www.bitchute.com/profile/4uBPC9RCH6e9/
And minds: https://www.minds.com/EnergyUnleashed
5:33
Making White Phosphorus -01 Testing the concept
basically a test run of a procedure i found which is a micro scale run to make White phos...
published: 27 Mar 2017
Making White Phosphorus -01 Testing the concept
Making White Phosphorus -01 Testing the concept
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- published: 27 Mar 2017
- views: 6388
basically a test run of a procedure i found which is a micro scale run to make White phosphorus. the original publisher cited this equation :
6NaPO3 + 10AI + 3Si02 = 3Na2Si03 + 5Al203 + 3P2
which was first published over a century ago by j.franck.
The publisher cited a 50% yield of 250mg out of the 500mg available P which was reportedly re sublimed to separate the white from the red P.
these two runs were basically a test run to prove the concept for myself and to see how the reaction proceeds before i scale it up with a steel retort . it seems to have worked very well and at a much lower temperature than i thought.
Experimental:
3g of a stochiometric ratio of sodium hexametaphosphate,
silicon dioxide and dark aluminium powder in slight excess were
well dried in an oven and mixed thoroughly in a plastic tub.
Exactly 3g of this mixture was placed in an 18mm Test tube
and this was sealed with a stopper which i had bored with two holes, one for argon to be inlet and one for a bent glass leading into cold water. paper toweling was wrapped around the tube and wet with ice water. the tube was then heated with a butane torch firstly and a MAPP torch for the second attempt.
the second attempt worked better.
I was able to get a little product recovered -i did not weigh it and watched it burn. but this was pretty much a test run with bigger and better attempts to come.
5:37
Cleaning the white Phosphorus.
All the white Phosphorus i have made so far was cleaned using similar methods to what is ...
published: 20 Jun 2017
Cleaning the white Phosphorus.
Cleaning the white Phosphorus.
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- published: 20 Jun 2017
- views: 6284
All the white Phosphorus i have made so far was cleaned using similar methods to what is used in industrial process- using dilute dichromate in acidic solutions.
i made a small solution of potassium dichromate with sulfuric acid and added some of this to the molten P4 while stirring the solution. The amount of dichromate solution and time it was immersed was quite arbitrary and i added as much as i thought i would need- a few mls and kept the cleaning going until i though it looked clean enough.
eventually it turned out much cleaner than i started, being a nice pale yellow colour rather than the red i started with.
Next i may do a video on converting some of this to red phosphorus.
maybe. it is becoming wintery here.
See more on Bitchute:
https://www.bitchute.com/profile/4uBPC9RCH6e9/
And minds: https://www.minds.com/EnergyUnleashed
Music:
Destination Unknown by Audionautix is licensed under a Creative Commons Attribution license (https://creativecommons.org/licenses/by/4.0/)
Artist: http://audionautix.com/
Impact Intermezzo by Kevin MacLeod is licensed under a Creative Commons Attribution license (https://creativecommons.org/licenses/by/4.0/)
Source: http://incompetech.com/music/royalty-free/index.html?isrc=USUAN1100620
Artist: http://incompetech.com/
0:26
Jawdropping Side by Side Trial with Genesis Ag Liberate
Jameson Quinn of Quinn Farms in Cove City, NC accidentally left Genesis Ag's Liberate off ...
published: 19 May 2016
Jawdropping Side by Side Trial with Genesis Ag Liberate
Jawdropping Side by Side Trial with Genesis Ag Liberate
- Report rights infringement
- published: 19 May 2016
- views: 2163
Jameson Quinn of Quinn Farms in Cove City, NC accidentally left Genesis Ag's Liberate off of 16 rows during the transplant process on April 4th. By May 19th the visual results in his field were almost unbelievable.
To learn more about Genesis Ag's liberate go here:
http://www.genesis.ag/products/liberate/
Trial
In law, a trial is a coming together of parties to a dispute, to present information (in the form of evidence) in a tribunal, a formal setting with the authority to adjudicate claims or disputes. One form of tribunal is a court. The tribunal, which may occur before a judge, jury, or other designated trier of fact, aims to achieve a resolution to their dispute.
Types of trial divided by the finder of fact
Where the trial is held before a group of members of the community, it is called a jury trial. Where the trial is held solely before a judge, it is called a bench trial.
Bench trials are often resolved faster. Furthermore, a favorable ruling for one party in a bench trial will frequently lead the other party to offer a settlement.
Hearings before administrative bodies may have many of the features of a trial before a court, but are typically not referred to as trials.
An appellate proceeding is also generally not deemed a trial, because such proceedings are usually restricted to review of the evidence presented before the trial court, and do not permit the introduction of new evidence.
This page contains text from Wikipedia, the Free Encyclopedia - https://wn.com/Trial
How To Make White Phosphorus (Trial 1)...
Making White Phosphorus- done it this time!...
Making White Phosphorus -01 Testing the concept...
Cleaning the white Phosphorus....
